Production Method 1

20138-79-8

79780-61-3

Reaction Conditions

1.1 Catalysts: Cobalt dichloride hexahydrate Solvents: Ethanol ,  Tetrahydrofuran ;  15 min, rt
1.2 Reagents: Sodium borohydride ;  reflux; 1.5 h, reflux

Reference

Photodriven Multi-electron Storage in Disubstituted RuII Dppz Analogues

Aslan, Joseph M.; et al, Chemistry - A European Journal, 2015, 21(48), 17314-17323

Production Method 2

273-13-2

79780-61-3

Reaction Conditions

1.1 Reagents: Bromine ,  Hydrogen bromide
2.1 Solvents: Dimethylformamide ;  3 h, reflux
3.1 Catalysts: Cobalt dichloride hexahydrate Solvents: Ethanol ,  Tetrahydrofuran ;  15 min, rt
3.2 Reagents: Sodium borohydride ;  reflux; 1.5 h, reflux

Reference

Photodriven Multi-electron Storage in Disubstituted RuII Dppz Analogues

Aslan, Joseph M.; et al, Chemistry - A European Journal, 2015, 21(48), 17314-17323

Production Method 3

20138-79-8

79780-61-3

Reaction Conditions

1.1 Reagents: Acetic acid ,  Iron ;  30 min, reflux; reflux → rt
1.2 Reagents: Sodium hydroxide Solvents: Water ;  basified, rt

Reference

Solution-Processable n-Type Semiconductors Based on Unsymmetrical Naphthalene Imides: Synthesis, Characterization, and Applications in Field-Effect Transistors

Shao, Jinjun; et al, Chemistry - An Asian Journal, 2014, 9(1), 253-260

Production Method 4

15155-41-6

79780-61-3

Reaction Conditions

1.1 Solvents: Dimethylformamide ;  3 h, reflux
2.1 Catalysts: Cobalt dichloride hexahydrate Solvents: Ethanol ,  Tetrahydrofuran ;  15 min, rt
2.2 Reagents: Sodium borohydride ;  reflux; 1.5 h, reflux

Reference

Photodriven Multi-electron Storage in Disubstituted RuII Dppz Analogues

Aslan, Joseph M.; et al, Chemistry - A European Journal, 2015, 21(48), 17314-17323

Production Method 5

79780-61-3

Reaction Conditions

1.1 Reagents: Thionyl chloride Solvents: Dichloromethane
2.1 Reagents: Bromine ,  Hydrogen bromide
3.1 Solvents: Dimethylformamide ;  3 h, reflux
4.1 Catalysts: Cobalt dichloride hexahydrate Solvents: Ethanol ,  Tetrahydrofuran ;  15 min, rt
4.2 Reagents: Sodium borohydride ;  reflux; 1.5 h, reflux

Reference

Photodriven Multi-electron Storage in Disubstituted RuII Dppz Analogues

Aslan, Joseph M.; et al, Chemistry - A European Journal, 2015, 21(48), 17314-17323

1,4-Benzenedicarbonitrile, 2,3-diamino- Raw materials

• BTD
• 2,1,3-Benzothiadiazole
• 4,7-Dibromo-2,1,3-benzothiadiazole

1,4-Benzenedicarbonitrile, 2,3-diamino- Preparation Products

• 1,4-Benzenedicarbonitrile, 2,3-diamino- (79780-61-3)

• 1. Acentric and chiral heterometallic inorganic–organic hybrid frameworks mediated by alkali or alkaline earth ions: synthesis and NLO properties
  Huabin Zhang,Shaowu Du CrystEngComm, 2014,16, 4059-4068
• 2. An aqueous ammonia sensor based on an inkjet-printed polyaniline nanoparticle-modified electrode
  Karl Crowley,Eimer O'Malley,Aoife Morrin,Malcolm R. Smyth,Anthony J. Killard Analyst, 2008,133, 391-399
• 3. An antioxidative galactomannan extracted from Chinese Sesbania cannabina enhances immune activation of macrophage cells?
  Chongyang Zhu,Xiaojia Bian,Xin Jia,Ning Tang,Yongqiang Cheng Food Funct., 2020,11, 10635-10644
• 4. An analyte-triggered artificial peroxidase system based on dimanganese complex for a versatile enzyme assay?
  Suji Lee,Min Su Han Chem. Commun., 2021,57, 9450-9453
• 5. Aggregation-induced emission enhancement in halochalcones?
  Patricia A. A. M. Vaz,Jo?o Rocha,Artur M. S. Silva New J. Chem., 2016,40, 8198-8201

• Solvents and Organic Chemicals Organic Compounds Benzenoids Benzene and substituted derivatives Benzonitriles

• 1885-29-6(Anthranilonitrile)
• 5925-93-9(2-Amino-5-methylbenzonitrile)
• 146351-93-1(Benzonitrile,2-amino-3,5-dimethyl-)
• 63069-52-3(2-Aminoisophthalonitrile)
• 326591-56-4(1,3-Benzenedicarbonitrile, 4,6-diamino-, radical ion(2+) (9CI))
• 60710-80-7(3-Amino-4-methylbenzonitrile)
• 26830-96-6(2-Amino-4-methylbenzonitrile)
• 14346-13-5(2,5-Diaminobenzonitrile)
• 18128-06-8(Benzonitrile,2,3,5,6-tetraamino-, hydrochloride (1:4))
• 79780-60-2(1,2-Benzenedicarbonitrile, 3,4-diamino-)