Production Method 1

24424-99-5

99-03-6

79537-70-5

Reaction Conditions

1.1 Solvents: Tetrahydrofuran ;  48 h, rt

Reference

Rational modification, synthesis and biological evaluation of 3,4-dihydroquinoxalin-2(1H)-one derivatives as potent and selective c-Jun N-terminal kinase 3 (JNK3) inhibitors

Dou, Xiaodong; Huang, Huixia; Jiang, Lan; Zhu, Guiwang; Jin, Hongwei; et al, European Journal of Medicinal Chemistry, 2020, 201,

Production Method 2

24424-99-5

99-03-6

79537-70-5

Reaction Conditions

1.1 Reagents: Triethylamine ,  Sodium carbonate Solvents: Tetrahydrofuran ,  Water ;  12 h, rt

Reference

Synthesis of thiourea and sulfonylurea derivatives of chalcones and flavones and their biological evaluation

Satyanarayana, Mavurapu; Shukla, Poonam; Tiwari, Priti; Tripathi, Brajendra K.; Srivastava, Arvind K.; et al, Indian Journal of Heterocyclic Chemistry, 2021, 31(3), 341-345

Production Method 3

24424-99-5

99-03-6

79537-70-5

Reaction Conditions

1.1 Solvents: 1,4-Dioxane ;  rt; 48 h, 80 °C

Reference

Novel Bcl-2 Inhibitors Selectively Disrupt the Autophagy-Specific Bcl-2-Beclin 1 Protein-Protein Interaction

Dong, Xiaonan; Liang, Qiren; Pan, Yun-Zu; Wang, Xiaoyu; Kuo, Yi-Chun; et al, ACS Medicinal Chemistry Letters, 2022, 13(9), 1510-1516

Production Method 4

24424-99-5

251966-49-1

79537-70-5

Reaction Conditions

1.1 Reagents: Poly(methylhydrosiloxane) Catalysts: Palladium dihydroxide Solvents: Ethanol ;  3 h, rt

Reference

Single-step conversion of N-benzyl, N-trityl and N-diphenylmethyl amines to t-butyl carbamates using polymethylhydrosiloxane

Chandrasekhar, S.; Babu, B. Nagendra; Reddy, Ch. Raji, Tetrahedron Letters, 2003, 44(10), 2057-2059

Production Method 5

4248-19-5

2142-63-4

79537-70-5

Reaction Conditions

1.1 Reagents: Cesium carbonate Catalysts: Palladium diacetate ,  X-Phos Solvents: 1,4-Dioxane ;  1.5 h, 100 °C; 100 °C → rt

Reference

Pd-catalyzed amidation of aryl(Het) halides with tert-butyl carbamate

Qin, Lijin; Cui, Hongmeng; Zou, Dapeng; Li, Jingya; Wu, Yangjie; et al, Tetrahedron Letters, 2010, 51(33), 4445-4448

Tert-butyl 3-acetylphenylcarbamate Raw materials

• Di-tert-butyl dicarbonate
• tert-Butyl carbamate
• 3'-Bromoacetophenone
• 1-(3-aminophenyl)ethan-1-one
• 1-(3-(Dibenzylamino)phenyl)ethanone

Tert-butyl 3-acetylphenylcarbamate Preparation Products

• Tert-butyl 3-acetylphenylcarbamate (79537-70-5)

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• 5. Acetyl group orientation modulates the electronic ground-state asymmetry of the special pair in purple bacterial reaction centers
  P. K. Wawrzyniak,M. T. P. Beerepoot,H. J. M. de Groot,F. Buda Phys. Chem. Chem. Phys., 2011,13, 10270-10279

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