Production Method 1

7098-07-9

512-56-1

7351-83-9

65039-03-4

Reaction Conditions

1.1 0.3 min, 150 °C

Reference

Microwave-assisted synthesis of ionic liquids of phosphate and application in Knoevenagel reaction

Lu, Xiangjun; Dou, Hui; Dai, Yaodong; Chen, Da, Nanjing Hangkong Hangtian Daxue Xuebao, 2009, 41(3), 414-417

Production Method 2

7098-07-9

512-56-1

7351-83-9

65039-03-4

Reaction Conditions

1.1 Solvents: Acetonitrile ;  6 d, 353 K

Reference

Formation and Substructure of Cellulose/Ionic Liquid Complex Crystals: Results from Wide-Angle X-ray Scattering and Solid-State 13C NMR Spectroscopy

Endo, Takatsugu ; Nakano, Takeru; Tokumasu, Nana; Kimura, Yoshifumi, Crystal Growth & Design, 2022, 22(12), 7603-7610

Production Method 3

7098-07-9

512-56-1

7351-83-9

65039-03-4

Reaction Conditions

1.1 12 h, 130 °C

Reference

Research on the degradation behaviors of wood pulp cellulose in ionic liquids

Wei, Jia; Gao, Hongshuai; Li, Yao; Nie, Yi, Journal of Molecular Liquids, 2022, 356,

Production Method 4

7098-07-9

512-56-1

7351-83-9

65039-03-4

Reaction Conditions

1.1 24 h, 80 °C

Reference

Development of Nanoscale Hybrids from Ionic Liquid-Peptide Amphiphile Assemblies as New Functional Materials

Daso, Rachel E.; Osborn, Luke J.; Thomas, Marie F.; Banerjee, Ipsita A., ACS Omega, 2020, 5(24), 14543-14554

Production Method 5

7098-07-9

512-56-1

7351-83-9

65039-03-4

Reaction Conditions

1.1 72 h, 80 °C

Reference

additive for lubricating oil comprising ionic liquid

, World Intellectual Property Organization, , ,

Production Method 6

7098-07-9

512-56-1

7351-83-9

65039-03-4

Reaction Conditions

1.1 1 h, 100 °C; 18 h, 80 °C

Reference

On the solubility of wood in non-derivatising ionic liquids

Kylloenen, Lasse; Parviainen, Arno; Deb, Somdatta; Lawoko, Martin; Gorlov, Mikhail; et al, Green Chemistry, 2013, 15(9), 2374-2378

Production Method 7

7098-07-9

512-56-1

7351-83-9

65039-03-4

Reaction Conditions

1.1 rt; rt → 80 °C; 24 h, 80 °C

Reference

Fast and efficient extraction of DNA from meat and meat derived products using aqueous ionic liquid buffer systems

Ressmann, Anna K.; Garcia, Eric Gonzalez; Khlan, Diana; Gaertner, Peter; Mach, Robert L.; et al, New Journal of Chemistry, 2015, 39(6), 4994-5002

Production Method 8

7098-07-9

512-56-1

7351-83-9

65039-03-4

Reaction Conditions

1.1 rt; rt → 80 °C; 24 h, 80 °C

Reference

Direct extraction of genomic DNA from maize with aqueous ionic liquid buffer systems for applications in genetically modified organisms analysis

Gonzalez Garcia, Eric; Ressmann, Anna K.; Gaertner, Peter; Zirbs, Ronald; Mach, Robert L.; et al, Analytical and Bioanalytical Chemistry, 2014, 406(30), 7773-7784

Production Method 9

7098-07-9

512-56-1

7351-83-9

65039-03-4

Reaction Conditions

1.1 24 h, 80 °C

Reference

Imidazolium dialkylphosphates-a class of versatile, halogen-free and hydrolytically stable ionic liquids

Kuhlmann, Esther; Himmler, Simone; Giebelhaus, Heidi; Wasserscheid, Peter, Green Chemistry, 2007, 9(3), 233-242

Production Method 10

7098-07-9

512-56-1

7351-83-9

65039-03-4

Reaction Conditions

1.1 12 h, 150 °C

Reference

Effects of water content on the dissolution behavior of wool keratin using 1-ethyl-3-methylimidazolium dimethylphosphate

Zhang, Zhenlei; Zhang, Xiaochun; Nie, Yi; Wang, Hui; Zheng, Shuangshuang; et al, Science China: Chemistry, 2017, 60(7), 934-941

Production Method 11

512-56-1

65039-08-9

7351-83-9

65039-03-4

Reaction Conditions

1.1 Solvents: Methyl isobutyl ketone ;  rt; 15 min, rt; rt → 110 °C; 12 h, 110 °C

Reference

Extraction of Polyhydroxyalkanoates from Purple Non-Sulfur Bacteria by Non-Chlorinated Solvents

Filippi, Sara ; Cinelli, Patrizia ; Mezzetta, Andrea ; Carlozzi, Pietro ; Seggiani, Maurizia, Polymers (Basel, 2021, 13(23),

Production Method 12

7098-07-9

512-56-1

7351-83-9

65039-03-4

Reaction Conditions

1.1 24 h, 80 °C

Reference

Dissolution capacity and rheology of cellulose in ionic liquids composed of imidazolium cation and phosphate anions

Zheng, Bingqian; Harris, Chaudhary; Bhatia, Surita R. ; Thomas, Marie F., Polymers for Advanced Technologies, 2019, 30(7), 1751-1758

Production Method 13

7098-07-9

512-56-1

7351-83-9

65039-03-4

Reaction Conditions

1.1 Solvents: Acetonitrile ;  6.5 h, 75 °C

Reference

Method for preparing imidazolium dialkyl phosphate ionic liquid

, China, , ,

Production Method 14

7098-07-9

512-56-1

7351-83-9

65039-03-4

Reaction Conditions

1.1 100 °C; 80 h, 120 °C

Reference

Screening of glycoside hydrolases and ionic liquids for fibre modification

Rahikainen, Jenni ; Anbarasan, Sasikala; Wahlstroem, Ronny; Parviainen, Arno; King, Alistair W. T.; et al, Journal of Chemical Technology and Biotechnology, 2018, 93(3), 818-826

Production Method 15

7098-07-9

512-56-1

7351-83-9

65039-03-4

Reaction Conditions

Reference

DBN-based ionic liquids with high capability for the dissolution of wool keratin

Liu, Xue; Nie, Yi; Meng, Xianglei; Zhang, Zhenlei; Zhang, Xiangping; et al, RSC Advances, 2017, 7(4), 1981-1988

Production Method 16

7098-07-9

512-56-1

7351-83-9

65039-03-4

Reaction Conditions

1.1 12 h, 423 K

Reference

Highly Efficient Dissolution of Wool Keratin by Dimethylphosphate Ionic Liquids

Zheng, Shuangshuang; Yi, Nie; Zhang, Suojiang; Zhang, Xiangping; Wang, Lijun, ACS Sustainable Chemistry & Engineering, 2015, 3(11), 2925-2932

Production Method 17

7098-07-9

512-56-1

7351-83-9

65039-03-4

Reaction Conditions

1.1 4 h, 120 °C; 18 h, 120 °C

Reference

Process for fibrillating lignocellulosic materials using ionic liquids

, World Intellectual Property Organization, , ,

Production Method 18

7098-07-9

512-56-1

7351-83-9

65039-03-4

Reaction Conditions

1.1 25 °C → 60 °C; 24 h, 60 °C

Reference

Ionic liquid for polysaccharide treatment

, Japan, , ,

Production Method 19

7098-07-9

512-56-1

7351-83-9

65039-03-4

Reaction Conditions

1.1 25 °C → 60 °C; 24 h, 60 °C
1.2 Solvents: Diethyl ether ;  60 °C; 6 h, 60 °C; 24 h, 80 °C

Reference

Treating agent for polysaccharide

, World Intellectual Property Organization, , ,

Dimethylphosphate Raw materials

• 1-Ethyl-1H-imidazole
• Trimethyl phosphate
• 1-Ethyl-3-methylimidazolium bromide

Dimethylphosphate Preparation Products

• Dimethylphosphate (7351-83-9)
• 1H-Imidazolium,3-ethyl-1-methyl- (65039-03-4)

• 1. Exceptionally high temperature spin crossover in amide-functionalised 2,6-bis(pyrazol-1-yl)pyridine iron(ii) complex revealed by variable temperature Raman spectroscopy and single crystal X-ray diffraction?
  Max Attwood,Hiroki Akutsu,Lee Martin,Toby J. Blundell,Pierre Le Maguere,Scott S. Turner Dalton Trans., 2021,50, 11843-11851
• 2. Fast-Track to Research Data Management in Experimental Material Science-Setting the Ground for Research Group Level Materials Digitalization.
  LarsBanko,AlfredLudwig
• 3. Excess electrons in lithium–ethylamine solutions—density, electrical conductivity and EPR studies
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• 4. Fe/Fe3C@C nanoparticles encapsulated in N-doped graphene–CNTs framework as an efficient bifunctional oxygen electrocatalyst for robust rechargeable Zn–air batteries?
  Zhiyan Chen,Nan Wu,Yaobing Wang,Bing Wang,Yingde Wang J. Mater. Chem. A, 2018,6, 516-526
• 5. EWOD-driven droplet microfluidic device integrated with optoelectronic tweezers as an automated platform for cellular isolation and analysis?
  Gaurav J. Shah,Eric P.-Y. Chiou,Ming C. Wu,Chang-Jin “CJ” Kim Lab Chip, 2009,9, 1732-1739

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