Production Method 1

47855-94-7

47855-94-7

823-96-1

Reaction Conditions

1.1 Reagents: Triphenylmethane Solvents: 1,2-Dichlorobenzene ;  2 atm, -78 °C; 24 h, 20 °C

Reference

Complete reductive cleavage of CO facilitated by highly electrophilic borocations

Curless, Liam D.; et al, Chemical Communications (Cambridge, 2015, 51(54), 10903-10906

Production Method 2

47855-94-7

47855-94-7

823-96-1

Reaction Conditions

1.1 Reagents: Triphenylmethane Solvents: 1,2-Dichlorobenzene ;  2 atm, -78 °C; 100 °C

Reference

Complete reductive cleavage of CO facilitated by highly electrophilic borocations

Curless, Liam D.; et al, Chemical Communications (Cambridge, 2015, 51(54), 10903-10906

Production Method 3

1722-26-5

47855-94-7

13948-08-8

47855-94-7

823-96-1

Reaction Conditions

1.1 Solvents: 1,2-Dichlorobenzene ,  DMSO-d6 ;  10 min, rt
2.1 Reagents: Triphenylmethane Solvents: 1,2-Dichlorobenzene ;  2 atm, -78 °C; 100 °C

Reference

Complete reductive cleavage of CO facilitated by highly electrophilic borocations

Curless, Liam D.; et al, Chemical Communications (Cambridge, 2015, 51(54), 10903-10906

Production Method 4

88996-23-0

47855-94-7

13948-08-8

47855-94-7

823-96-1

Reaction Conditions

1.1 Solvents: 1,2-Dichlorobenzene ,  DMSO-d6 ;  10 min, rt
2.1 Reagents: Triphenylmethane Solvents: 1,2-Dichlorobenzene ;  2 atm, -78 °C; 24 h, 20 °C

Reference

Complete reductive cleavage of CO facilitated by highly electrophilic borocations

Curless, Liam D.; et al, Chemical Communications (Cambridge, 2015, 51(54), 10903-10906

Raw materials

• Borane N,\u200bN-\u200bDiisopropylethylamin\u200be Complex
• Borane Triethylamine Complex
• Methylium, triphenyl-

Preparation Products

• Trimethylboroxin (823-96-1)
• (47855-94-7)

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