Production Method 1

15515-54-5

33974-40-2

Reaction Conditions

1.1 Reagents: Iodobenzene diacetate Solvents: Methanol ;  10 - 15 min, 273.15 K
1.2 Reagents: Sodium hydroxide ,  Monopotassium phosphate Solvents: Water ;  pH 7, rt

Reference

Photooxygenation of masked o-benzoquinones: an efficient entry into highly functionalized cyclopentenones from 2-methoxyphenols

Kao, Tzu-Chiao; Chuang, Gary Jing; Liao, Chun-Chen, Angewandte Chemie, 2008, 47(38), 7325-7327

Production Method 2

16373-02-7

33974-40-2

2300-74-5

37942-07-7

Reaction Conditions

1.1 Reagents: Copper ,  Oxygen Catalysts: Cuprous chloride Solvents: Methanol

Reference

I. Catalytic oxidation of 2-(hydroxymethyl)phenols with the systems MnCln/M0/O2 (M = copper, iron)

Sparfel, Daniel; Baranne-Lafont, Joele; Nguyen Kim Cuong; Capdevielle, Patrice; Maumy, Michel, Tetrahedron, 1990, 46(3), 793-802

2,4-Cyclohexadien-1-one, 2,4-bis(1,1-dimethylethyl)-6,6-dimethoxy- Raw materials

• Benzenemethanol, 3,5-bis(1,1-dimethylethyl)-2-hydroxy-
• Phenol, 2,4-bis(1,1-dimethylethyl)-6-methoxy-

2,4-Cyclohexadien-1-one, 2,4-bis(1,1-dimethylethyl)-6,6-dimethoxy- Preparation Products

• 2,5-Cyclohexadiene-1,4-dione, 2-(1,1-dimethylethyl)-6-methoxy- (2300-74-5)
• 2,4-Cyclohexadien-1-one, 2,4-bis(1,1-dimethylethyl)-6,6-dimethoxy- (33974-40-2)
• 3,5-Di-t-butyl-2-hydroxybenzaldehyde (37942-07-7)

• 1. Enabling shape memory and healable effects in a conjugated polymer by incorporating siloxane via dynamic imine bond?
  Yaling Zhang,Chunhui Dai,Shiwei Zhou,Bin Liu Chem. Commun., 2018,54, 10092-10095
• 2. Emerging investigator series: heterogeneous reactions of sulfur dioxide on mineral dust nanoparticles: from single component to mixed components?
  Tao Wang,Yangyang Liu,Yue Deng,Hongbo Fu,Jianmin Chen Environ. Sci.: Nano, 2018,5, 1821-1833
• 3. Emergence of cationic polyamine dendrimersomes: design, stimuli sensitivity and potential biomedical applications
  Partha Laskar,Christine Dufès Nanoscale Adv., 2021,3, 6007-6026
• 4. Dissociation of large gaseous serine clusters produces abundant protonated serine octamer
  Jacob S. Jordan,Evan R. Williams Analyst, 2021,146, 2617-2625
• 5. Excellent electrochemical performance of LiFe0.4Mn0.6PO4 microspheres produced using a double carbon coating process?
  Yong Ping Huang,Tao Tao,Zheng Chen,Wei Han,Ying Wu,Chunjiang Kuang,Shaoxiong Zhou,Ying Chen J. Mater. Chem. A, 2014,2, 18831-18837

• 2098070-20-1(2-(3-(Pyridin-3-yl)-1H-pyrazol-1-yl)acetimidamide)
• 2680771-01-9(4-cyclopentyl-3-{(prop-2-en-1-yloxy)carbonylamino}butanoic acid)
• 1444113-98-7(N-(3-cyanothiolan-3-yl)-2-[(2,2,2-trifluoroethyl)sulfanyl]pyridine-4-carboxamide)
• 332062-08-5(Fmoc-S-3-amino-4,4-diphenyl-butyric acid)
• 1270529-38-8(1,2,3,4,5,6-Hexahydro-[2,3]bipyridinyl-6-ol)
• 941977-17-9(N'-(3-chloro-2-methylphenyl)-N-2-(dimethylamino)-2-(naphthalen-1-yl)ethylethanediamide)
• 2138166-62-6(2,2-Difluoro-3-[methyl(2-methylbutyl)amino]propanoic acid)
• 89640-58-4(2-Iodo-4-nitrophenylhydrazine)
• 1449132-38-0(3-Fluoro-5-(2-fluoro-5-methylbenzylcarbamoyl)benzeneboronic acid)
• 2034271-14-0(2-(1H-indol-3-yl)-N-{[6-(thiophen-2-yl)-[1,2,4]triazolo[4,3-b]pyridazin-3-yl]methyl}acetamide)