Cas no 2227068-13-3 (Phenylmethyl N-[5-[[2,3-bis-O-(phenylmethyl)-4,6-O-[(S)-phenylmethylene]-β-D-galactopyranosyl]oxy]pentyl]carbamate)

Phenylmethyl N-[5-[[2,3-bis-O-(phenylmethyl)-4,6-O-[(S)-phenylmethylene]-β-D-galactopyranosyl]oxy]pentyl]carbamate structure
2227068-13-3 structure
Product Name:Phenylmethyl N-[5-[[2,3-bis-O-(phenylmethyl)-4,6-O-[(S)-phenylmethylene]-β-D-galactopyranosyl]oxy]pentyl]carbamate
CAS No:2227068-13-3
MF:C40H45NO8
MW:667.787212133408
CID:6624940
Update Time:2024-01-19

Phenylmethyl N-[5-[[2,3-bis-O-(phenylmethyl)-4,6-O-[(S)-phenylmethylene]-β-D-galactopyranosyl]oxy]pentyl]carbamate Chemical and Physical Properties

Names and Identifiers

    • Phenylmethyl N-[5-[[2,3-bis-O-(phenylmethyl)-4,6-O-[(S)-phenylmethylene]-β-D-galactopyranosyl]oxy]pentyl]carbamate
    • Inchi： 1S/C40H45NO8/c42-40(47-28-32-20-10-3-11-21-32)41-24-14-5-15-25-43-39-37(45-27-31-18-8-2-9-19-31)36(44-26-30-16-6-1-7-17-30)35-34(48-39)29-46-38(49-35)33-22-12-4-13-23-33/h1-4,6-13,16-23,34-39H,5,14-15,24-29H2,(H,41,42)/t34-,35+,36+,37-,38+,39-/m1/s1
    • InChI Key： YKYPBVQXSSFEJA-GRPVOWEESA-N
    • SMILES： C(OCC1=CC=CC=C1)(=O)NCCCCCO[C@@H]1O[C@@H]2CO[C@@H](O[C@@H]2[C@H](OCC2=CC=CC=C2)[C@H]1OCC1=CC=CC=C1)C1=CC=CC=C1

Experimental Properties

  • Density: 1.23±0.1 g/cm3(Temp: 20 °C; Press: 760 Torr)(Predicted)
  • Boiling Point: 786.6±60.0 °C(Predicted)
  • pka: 12.68±0.46(Predicted)

Phenylmethyl N-[5-[[2,3-bis-O-(phenylmethyl)-4,6-O-[(S)-phenylmethylene]-β-D-galactopyranosyl]oxy]pentyl]carbamate Production Method

Production Method 1

Reaction Conditions
1.1 Reagents: Sodium hydride Solvents: Dimethylformamide ;  0 °C; overnight, rt
1.2 Reagents: Water ;  0 °C
2.1 Reagents: Tosyl chloride ,  Silver triflate Solvents: Dichloromethane ;  3 h, rt
2.2 Solvents: Dichloromethane ;  1 h
Reference
Simple and Practical Real-Time Analysis of Solid-Phase Reactions by Thin-Layer Chromatography
Wu, Chia-Hui; et al, Synlett, 2018, 29(11), 1430-1436

Production Method 2

Reaction Conditions
1.1 Reagents: Tosyl chloride ,  Silver triflate Solvents: Dichloromethane ;  3 h, rt
1.2 Solvents: Dichloromethane ;  1 h
Reference
Simple and Practical Real-Time Analysis of Solid-Phase Reactions by Thin-Layer Chromatography
Wu, Chia-Hui; et al, Synlett, 2018, 29(11), 1430-1436

Production Method 3

Reaction Conditions
1.1 Catalysts: Camphorsulfonic acid Solvents: Acetonitrile ;  overnight, rt
1.2 Reagents: Trimethylamine ;  rt
2.1 Reagents: Sodium hydride Solvents: Dimethylformamide ;  0 °C; overnight, rt
2.2 Reagents: Water ;  0 °C
3.1 Reagents: Tosyl chloride ,  Silver triflate Solvents: Dichloromethane ;  3 h, rt
3.2 Solvents: Dichloromethane ;  1 h
Reference
Simple and Practical Real-Time Analysis of Solid-Phase Reactions by Thin-Layer Chromatography
Wu, Chia-Hui; et al, Synlett, 2018, 29(11), 1430-1436

Phenylmethyl N-[5-[[2,3-bis-O-(phenylmethyl)-4,6-O-[(S)-phenylmethylene]-β-D-galactopyranosyl]oxy]pentyl]carbamate Raw materials

Phenylmethyl N-[5-[[2,3-bis-O-(phenylmethyl)-4,6-O-[(S)-phenylmethylene]-β-D-galactopyranosyl]oxy]pentyl]carbamate Preparation Products

Phenylmethyl N-[5-[[2,3-bis-O-(phenylmethyl)-4,6-O-[(S)-phenylmethylene]-β-D-galactopyranosyl]oxy]pentyl]carbamate Related Literature

2227068-13-3 (Phenylmethyl N-[5-[[2,3-bis-O-(phenylmethyl)-4,6-O-[(S)-phenylmethylene]-β-D-galactopyranosyl]oxy]pentyl]carbamate) Related Products

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