Production Method 1

50-99-7

2138864-37-4

822-36-6

1400563-39-4

160818-32-6

13925-07-0

15707-23-0

872-82-2

109-08-0

19141-85-6

Reaction Conditions

1.1 Reagents: Ammonia Catalysts: Tungstate (W12(OH)2O386-), ammonium, hydrate (1:6:?) Solvents: Water ;  15 min, 180 °C

Reference

One-Step Synthesis of N-Heterocyclic Compounds from Carbohydrates over Tungsten-Based Catalysts

Chen, Xi; et al, ACS Sustainable Chemistry & Engineering, 2017, 5(11), 11096-11104

2,3-Dimethyl-6-(1Z)-1-propen-1-ylpyridine Raw materials

• D(+)-Glucose

2,3-Dimethyl-6-(1Z)-1-propen-1-ylpyridine Preparation Products

• 4-Methylimidazole (822-36-6)
• 2-Pyrazinemethanol, 3,5-dimethyl- (1400563-39-4)
• (3-Methylpyrazin-2-yl)methanol (160818-32-6)
• 3,5-Dimethyl-2-ethylpyrazine (13925-07-0)
• 2-Ethyl-3-methylpyrazine (15707-23-0)
• 2-(1H-imidazol-4-yl)ethan-1-ol (872-82-2)
• 2,3-Dimethyl-6-(1Z)-1-propen-1-ylpyridine (2138864-37-4)
• 2-Methylpyrazine (109-08-0)
• 4-ethyl-1H-imidazole (19141-85-6)

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  Amandine Altmayer-Henzien,Valérie Declerck,David J. Aitken,Ewen Lescop,Denis Merlet,Jonathan Farjon Org. Biomol. Chem., 2013,11, 7611-7615
• 5. Emerging investigator series: heterogeneous reactions of sulfur dioxide on mineral dust nanoparticles: from single component to mixed components?
  Tao Wang,Yangyang Liu,Yue Deng,Hongbo Fu,Jianmin Chen Environ. Sci.: Nano, 2018,5, 1821-1833

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