Production Method 1

604-35-3

19317-90-9

809-51-8

Reaction Conditions

1.1 Reagents: tert-Butyl hydroperoxide ,  Water Catalysts: Manganese oxide (MnO2) Solvents: Dichloromethane ;  -30 °C; 2 h, -30 °C; -30 °C → -10 °C; 15 h, -10 °C; 5 h, reflux

Reference

MnO2/TBHP: A Versatile and User-Friendly Combination of Reagents for the Oxidation of Allylic and Benzylic Methylene Functional Groups

Serra, Stefano, European Journal of Organic Chemistry, 2015, 2015(29), 6472-6478

3-Ac-(3beta,7alpha)-Cholest-5-ene-3,7-diol, Raw materials

• Cholesterol 3-Acetate

3-Ac-(3beta,7alpha)-Cholest-5-ene-3,7-diol, Preparation Products

• 3-Ac-(3beta,7alpha)-Cholest-5-ene-3,7-diol, (19317-90-9)
• 7-Oxo Cholesterol 3-Acetate (809-51-8)

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• Solvents and Organic Chemicals Organic Compounds Lipids and lipid-like molecules Steroids and steroid derivatives Cholesteryl esters
• Solvents and Organic Chemicals Organic Compounds Lipids and lipid-like molecules Steroids and steroid derivatives Steroid esters Cholesteryl esters

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