Production Method 1

1345977-93-6

170656-93-6

959058-28-7

87532-69-2

Reaction Conditions

1.1 Solvents: Toluene-d8 ;  2 d, 80 °C; 1 h, 80 °C → 100 °C; 5 h, 100 °C

Reference

Reduction of CO2 and SO2 with low valent nickel compounds under mild conditions

Gonzalez-Sebastian, Lucero; et al, Dalton Transactions, 2011, 40(36), 9116-9122

Production Method 2

130777-67-2

170656-93-6

959058-28-7

87532-69-2

Reaction Conditions

1.1 Solvents: Toluene ;  1 h, rt; 5 d, 65 °C
2.1 Solvents: Toluene-d8 ;  2 d, 80 °C; 1 h, 80 °C → 100 °C; 5 h, 100 °C

Reference

Reduction of CO2 and SO2 with low valent nickel compounds under mild conditions

Gonzalez-Sebastian, Lucero; et al, Dalton Transactions, 2011, 40(36), 9116-9122

Raw materials

• Nickel, bis[1,1'-(1,2-ethanediyl)bis[1,1-bis(1-methylethyl)phosphine-κP]]di-μ-hydrodi-, (Ni-Ni)

Preparation Products

• [2-[Bis(1-methylethyl)phosphino]ethyl]bis(1-methylethyl)phosphine oxide (959058-28-7)
• (170656-93-6)
• Phosphine, 1,2-ethanediylbis[bis(1-methylethyl)- (87532-69-2)

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