Production Method 1

534-13-4

12081-18-4

1699767-58-2

Reaction Conditions

1.1R:MgSO4, S:Me(CH2)4CH2OH, 20 min, 185°C
2.1R:K, S:96-47-9, 20 h, 100°C; cooled
3.1S:PhMe, 20 min, -25°C; 1 h, -25°C; -25°C → rt; 1.5 h, rt

Reference

Synthesis of an [(NHC)2Pd(SiMe3)2] Complex and Catalytic cis-Bis(silyl)ations of Alkynes with Unactivated Disilanes

By Ansell, Melvyn B. et al, Angewandte Chemie, 2015, 54(19), 5578-5582

Palladium, chloro(1,3-dihydro-1,3,4,5-tetramethyl-2H-imidazol-2-ylidene)[(1,2,3-η)-2-methyl-2-propen-1-yl]- Raw materials

• N,N'-Dimethylthiourea
• Palladium, di-m-chlorobis[(1,2,3-h)-2-methyl-2-propen-1-yl]di-

Palladium, chloro(1,3-dihydro-1,3,4,5-tetramethyl-2H-imidazol-2-ylidene)[(1,2,3-η)-2-methyl-2-propen-1-yl]- Preparation Products

• Palladium, chloro(1,3-dihydro-1,3,4,5-tetramethyl-2H-imidazol-2-ylidene)[(1,2,3-η)-2-methyl-2-propen-1-yl]- (1699767-58-2)

• 1. Fatty acid positional distribution in colostrum and mature milk of women living in Inner Mongolia, North Jiangsu and Guangxi of China?
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  Tengfei Yu,Yuehan Wu,Wei Li,Bin Li RSC Adv., 2014,4, 34134-34143
• 4. Enabling stable MnO2 matrix for aqueous zinc-ion battery cathodes?
  Yiding Jiao,Liqun Kang,Jasper Berry-Gair,Kit McColl,Jianwei Li,Haobo Dong,Hao Jiang,Ryan Wang,Furio Corà,Dan J. L. Brett,Ivan P. Parkin J. Mater. Chem. A, 2020,8, 22075-22082
• 5. Embedding heteroatoms: an effective approach to create porphyrin-based functional materials
  Norihito Fukui,Keisuke Fujimoto,Hideki Yorimitsu,Atsuhiro Osuka Dalton Trans., 2017,46, 13322-13341

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