Production Method 1

154445-77-9

1202179-48-3

91000-69-0

Reaction Conditions

1.1 Reagents: Diisopropylcarbodiimide Catalysts: 4-(Dimethylamino)pyridine Solvents: Dimethylformamide ;  1 min, rt; 1 h, rt
1.2 Reagents: Acetic anhydride Catalysts: 4-(Dimethylamino)pyridine Solvents: Dimethylformamide ;  30 min, rt
1.3 Reagents: Trifluoroacetic acid ,  Triisopropylsilane Solvents: Water ;  2 h, rt

Reference

Synthesis of an arginine tagged [Cys154-Arg180] fragment of NY-ESO-1: elimination of an undesired by-product using 'in house' resins

Harris, Paul W. R.; Brimble, Margaret A., Synthesis, 2009, (20), 3460-3466

Fmoc-Arg-HMBA-Arg6-OH Raw materials

• Fmoc-Arg(Pbf)-OH

Fmoc-Arg-HMBA-Arg6-OH Preparation Products

• Fmoc-Arg-OH (91000-69-0)
• Fmoc-Arg-HMBA-Arg6-OH (1202179-48-3)

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