Production Method 1

1186-79-4

80-58-0

Reaction Conditions

1.1 Reagents: Lithium diisopropylamide Solvents: Tetrahydrofuran ;  5 °C → 40 °C; 30 - 40 min, 35 - 40 °C; 40 °C → 25 °C
1.2 Reagents: N-Bromo-N-ethylethanamine Solvents: Tetrahydrofuran ;  2 h, 20 - 25 °C
1.3 Reagents: Hydrochloric acid Solvents: Water ;  pH 1

Reference

Reactions of α-carbanions of lithium acylates with N,N-diethyl-N-chloro- and N,N-diethyl-N-bromoamines

Zorin, A. V.; et al, Russian Journal of General Chemistry, 2016, 86(11), 2469-2472

Production Method 2

1186-79-4

80-58-0

Reaction Conditions

1.1 Reagents: N-Bromo-N-ethylethanamine Solvents: Tetrahydrofuran ;  2 h, 20 - 25 °C
1.2 Reagents: Hydrochloric acid Solvents: Water ;  pH 1

Reference

Reactions of α-carbanions of lithium acylates with N,N-diethyl-N-chloro- and N,N-diethyl-N-bromoamines

Zorin, A. V.; et al, Russian Journal of General Chemistry, 2016, 86(11), 2469-2472

2,3-diethylsuccinic acid Preparation Products

• 2,3-diethylsuccinic acid (1186-79-4)
• 2-Bromobutyric acid (80-58-0)

• 1. NMR conformational study of the neutralisation of meso- and rac-2,3-dimethyl- and 2,3-diethylsuccinic acids in aqueous solution
  Hartmut Komber J. Chem. Soc. Perkin Trans. 2 1995 1923
• 2. Radical-nucleophilic substitution (SRN1) reactions. Part 7.1 Reactions of aliphatic α-substituted nitro compounds.
  Suleiman I. Al-Khalil,W. Russell Bowman,Katherine Gaitonde,Madeleine A. Marley (née Nagel),Geoffrey D. Richardson J. Chem. Soc. Perkin Trans. 2 2001 1557
• 3. Contents pages
  J. Chem. Soc. Perkin Trans. 2 1995 P105
• 4. Flash vacuum pyrolysis of the 3-thiabicyclo[3.2.0]heptane 3,3-dioxide ring system: a new stereospecific synthesis of cis-1,2-divinyl derivatives
  J. I. G. Cadogan,Ian Gosney,Leo M. McLaughlin,Brendan J. Hamill J. Chem. Soc. Chem. Commun. 1980 1242
• 5. Contents pages
  J. Chem. Soc. Perkin Trans. 2 1995 P077

• Solvents and Organic Chemicals Organic Compounds Lipids and lipid-like molecules Fatty Acyls Branched fatty acids
• Solvents and Organic Chemicals Organic Compounds Lipids and lipid-like molecules Fatty Acyls Fatty acids and conjugates Branched fatty acids

• 595-37-9(Dimebutic acid)
• 610-09-3(cis-1,2-Cyclohexanedicarboxylic acid)
• 626-51-7(3-Methylglutaric acid)
• 619-81-8(Cis-1,2-Cyclohexanedicarboxylic Acid)
• 97-61-0(2-Methyl-pentanoic Acid)
• 498-21-5(Methylsuccinic acid)
• 124-83-4((1R,3S)-Camphoric Acid)
• 619-82-9(trans-cyclohexane-1,4-dicarboxylic acid)
• 105-43-1(3-methylpentanoic acid)
• 99-66-1(Valproic acid)