Production Method 1

696-62-8

117968-06-6

855-38-9

Reaction Conditions

1.1 Reagents: Triethylamine ,  Tetraphosphorus Catalysts: Iridium(1+), [4,4′-bis(1,1-dimethylethyl)-2,2′-bipyridine-κN1,κN1′]bis[2-(2-pyri… Solvents: Benzene ,  Acetonitrile ;  18 h, rt

Reference

Direct catalytic transformation of white phosphorus into arylphosphines and phosphonium salts

Lennert, Ulrich; et al, Nature Catalysis, 2019, 2(12), 1101-1106

Production Method 2

696-62-8

117968-06-6

855-38-9

Reaction Conditions

1.1 Reagents: Triethylamine ,  Sodium phosphide (Na(H2P)) Catalysts: Iridium(1+), [4,4′-bis(1,1-dimethylethyl)-2,2′-bipyridine-κN1,κN1′]bis[2-(2-pyri… Solvents: Acetonitrile ;  24 h, rt

Reference

Photocatalytic Arylation of P4 and PH3: Reaction Development Through Mechanistic Insight

Rothfelder, Robin; et al, Angewandte Chemie, 2021, 60(46), 24650-24658

Phosphonium, tetrakis(4-methoxyphenyl)-, iodide Raw materials

• 4-Iodoanisole

Phosphonium, tetrakis(4-methoxyphenyl)-, iodide Preparation Products

• Phosphonium, tetrakis(4-methoxyphenyl)-, iodide (117968-06-6)
• Tris(4-methoxyphenyl)phosphine (855-38-9)

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